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요약정보
异丙醇铝水解缩聚动力学 / Kinetic Analysis of Aluminum Isopropoxide Hydrolysis-Condensation
Resource Type
Academic Journal
Authors
卢杨
;
王晶
;
史忠祥
;
戴丽静
;
孙子婷
;
张洪铭
;
陈军军
;
LU Yang
;
WANG Jing
;
SHI Zhongxiang
;
DAI Lijing
;
SUN Ziting
;
ZHANG Hongming
;
CHEN Junjun
Source
化学反应工程与工艺 / Chemical Reaction Engineering and Technology
. 35(3):218-281
Subject
异丙醇铝
水解缩聚
动力学
Language
Chinese
ISSN
1001-7631
Online Access
Scopus
Find it @ DONGA
초록
利用水含量在线测定实验与计算机模拟相结合的方法研究了异丙醇铝水解-缩聚动力学.通过对不同异丙醇铝和水物质的量之比和不同温度下反应获得的水含量随时间变化曲线进行分析,采用非线性拟合方法分别求得异丙醇铝水解、脱水和脱醇缩聚的反应速率常数及活化能.利用实验结果及建立动力学模型,由龙格库塔法计算异丙醇铝的水解缩聚过程,并求得不同反应温度和初始反应物浓度比条件下各官能团浓度与反应终止时间的关系,进而获得反应终止时间与反应温度、初始反应物异丙醇铝浓度、异丙醇铝和水物质的量之比之间的关系方程,为制备低成本高纯氧化铝提供有价值的参考.
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