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요약정보
葡萄果实中10种氨基甲酸酯类农药的快速测定 / Rapid Determination of Ten Carbamate Pesticides in Grape
Resource Type
Academic Journal
Authors
孙蕾
;
韩瑨烜
;
梁秋艳
;
SUN Lei
;
HAN Jinxuan
;
LIANG Qiuyan
Source
中外葡萄与葡萄酒 / Sino-Overseas Grapevine & Wine
. (1):52-55
Subject
葡萄果实
氨基甲酸酯
农药残留
快速测定
Language
Chinese
ISSN
1004-7360
Online Access
Find it @ DONGA
초록
为提高葡萄果实中氨基甲酸酯类农药的检测效率,建立了高效液相色谱柱后衍生法快速测定克百威等10种氨基甲酸酯类农药残留量的方法.结果表明,在0.05~2.00μg·mL-1线性范围内,10种农药浓度对应峰面积有良好的线性关系,相关系数均大于0.9990,检出限为0.009~0.010μg·mL-1,添加回收率为77%~104%,相对标准偏差在1.1%~6.5%.本方法前处理简单,灵敏度高,检出限低,操作实用性强,能够为有效控制葡萄质量安全提供可靠的技术保障.
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