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요약정보
电感耦合等离子体原子发射光谱法测定电解金属锰中磷、硅、硒、铁
Resource Type
Academic Journal
Authors
孙红敬
;
庞振兴
;
闫丽
;
腰瑞雪
;
刘佳
;
焦丽
Source
中国检验检测 / China Inspection Body&Laboratory
. 31(5):50-53
Subject
电感耦合等离子体原子发射光谱法
电解金属锰
硅
铁
硒
磷
Language
Chinese
ISSN
1673-8764
Online Access
Find it @ DONGA
초록
本文提出了一种电感耦合等离子体原子发射光谱法同时测定电解金属锰中硅、铁、硒、磷的方法.试样经硝酸、盐酸处理,以高纯二氧化锰为基体绘制工作曲线,通过调整仪器测量条件,同时测定电解金属锰中硅、铁、硒、磷元素.对试样的处理方法、仪器的测量条件、基体等进行了实验,建立了系统的分析方法,并对试样的精密度、回收率做了实验,结果显示,说明方法相对标准偏差<5.0%,回收率在 95%~105%之间.本方法简便快速,准确可靠,提高了日常检化验效率,对实际生产具有重要意义.
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