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요약정보
胆木浸膏糖浆质量标准研究 / Study on quality standard of Danmu extract syrup
Resource Type
Academic Journal
Authors
李湘怡
;
周明艳
;
谢振蕊
;
李丽
;
刘爱霞
;
张钰昕
;
赖伟勇
;
张俊清
;
关薇薇
;
LI Xiang-yi
;
ZHOU Ming-yan
;
XIE Zhen-rui
;
LI Li
;
LIU Ai-xia
;
ZHANG Yu-xin
;
LAI Wei-yong
;
ZHANG Jun-qin
;
GUAN Wei-wei
Source
海南医学院学报 / Journal of Hainan Medical University
. 27(9):651-660
Subject
胆木浸膏糖浆
质量标准
异长春花内酰胺
绿原酸
高效液相色谱法
薄层色谱法
Language
Chinese
ISSN
1007-1237
Online Access
Find it @ DONGA
초록
目的:建立中药制剂胆木浸膏糖浆的质量标准.方法:采用薄层色谱法对胆木浸膏糖浆中胆木进行定性鉴别;采用高效液相色谱法测定胆木中的异长春花苷内酰胺和绿原酸的含量.结果:胆木薄层色谱鉴别斑点清晰、无阴性干扰.异长春花苷内酰胺在100~300μg/mL范围内线性关系良好(R2=0.9997),平均回收率为99.1%,RSD为1.16%(n=9);绿原酸在6.7~20.2μg/mL范围内线性关系良好(R2=0.9991),平均回收率为99.9%,RSD为1.10%(n=9).结论:制定的胆木浸膏糖浆质量标准安全合理,方法简便,且准确性、重现性较好,可用于胆木浸膏糖浆的质量控制.
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