Self-compacting concrete is highly advanced concrete with much higher fluidity without segregation, bleeding and it is suitable for placing in structures with congested reinforcement of structure like Vierendeel truss under its self-weight without vibration. Mix proportion of self-compacting concrete must ensure a good balance between deformability and stability. Behavior of concrete can be affected by the characteristics of selected ingredients in concrete and the mix proportions. It becomes necessary to evolve a procedure for mix design of SCC. The paper presents an experimental procedure for the mix design of self-compacting concrete for grade M60 and implementation of the same mix at cast in situ heavily dense reinforcement structure-Vierendeel truss of Sitabuldi Metro Station in Nagpur Metro Project. The test results for acceptance characteristics of M60 grade self-compacting concrete such as slump flow, V-funnel, L-box, compressive strength at the ages of 7, 28, and 56 days determined, and results are included here. Successful production of temperature control self-compacting concrete from batching plant, transportation and placement procedures and proper planning of handling and execution of self-compacting concrete at site are presented in this article.