Study on synthesis of dl-monopivalyl gylcerol ester
- Resource Type
- Conference
- Authors
- Zhen, Xiao-Li; Han, Jian-Rong; Tian, Xia; Lei, Guang-Hua; Liu, Shou-Xi
- Source
- 2011 International Conference on Consumer Electronics, Communications and Networks (CECNet) Consumer Electronics, Communications and Networks (CECNet), 2011 International Conference on. :1719-1721 Apr, 2011
- Subject
- Communication, Networking and Broadcast Technologies
Components, Circuits, Devices and Systems
Computing and Processing
Engineered Materials, Dielectrics and Plasmas
Power, Energy and Industry Applications
Signal Processing and Analysis
Compounds
Solids
Industries
Saturation magnetization
Pharmaceuticals
Magnetic liquids
Educational institutions
Pivalyl Chloride
Gylcerol
dl-gylcerol monoester of pivalic acid
alcoholysis
Synthesis
- Language
dl-Gylcerol monoester of pivalic acid was synthesized by alcoholysis reaction of pivalyl chloride with acetone ketal of glycerine. The effect of molar ratio, reaction time, reaction temperature and catalyst dosage on the yield was investigated. The product structure was characterized by IR and 1 HNMR. Results indicated that yield of dl-gylcerol monoester of pivalic acid reached 75.5% at 25°C and 6h under the condition of p-toluenesulfonic acid as catalyst.